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工藝氣中痕量硫化物測定毛細(xì)管柱
工藝氣中痕量硫化物測定毛細(xì)管柱 詳細(xì)信息：

名稱：毛細(xì)管柱

固定相：專用

規(guī)格：30m*0.53mm

型號：HH-Sulfur-30

焦?fàn)t氣制取LNG生產(chǎn)過程中需嚴(yán)格控制合成氣中的硫含量,以期增加合成催化劑的使用壽命。
浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司采用氣相色譜儀-硫化學(xué)發(fā)光檢測器(GC-SCD)方法,測定了焦?fàn)t氣制LNG過程中痕量形態(tài)硫化物及總硫含量,并結(jié)合實際,討論了分析過程中需注意的問題。標(biāo)準(zhǔn)氣校準(zhǔn),計算各種組分的檢出限均低于10.00×10-9(體積分?jǐn)?shù)),總硫含量33.00×10-9。含硫組分的標(biāo)準(zhǔn)曲線相關(guān)性均優(yōu)于0.996。相對標(biāo)準(zhǔn)偏差(RSD,N=7)均小于7%。合成氣樣品測定過程中,在接近檢出限的情況下,相對標(biāo)準(zhǔn)偏差小于12%。本方法可很好地滿足工廠生產(chǎn)控制的需要。

硫化氫，羰基硫，二氧化硫，二硫化碳，柱效高，分離好，結(jié)果滿意。


工藝氣中痕量硫化物測定毛細(xì)管柱 測試譜圖：




Capillary Column for the Determination of Trace Sulfide in Process Gas
Capillary column for determination of trace sulfide in process gas Details:

Name: Capillary Column

Stationary phase: dedicated

Specification: 30m*0.53mm

Model: HH-Sulfur-30



In the production process of coke oven gas to LNG, the sulfur content in the synthesis gas needs to be strictly controlled in order to increase the service life of the synthesis catalyst.
Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. used the gas chromatograph-sulfur chemiluminescence detector (GC-SCD) method to determine the trace sulfide and total sulfur content in the process of coke oven gas to LNG, and combined with actual conditions, Discuss the problems that need to be paid attention to in the analysis process. Standard gas calibration, calculated that the detection limits of various components are lower than 10.00×10-9 (volume fraction), and the total sulfur content is 33.00×10-9. The correlation of the standard curve of sulfur-containing components is better than 0.996. The relative standard deviations (RSD, N=7) were all less than 7%. In the process of synthetic gas sample determination, the relative standard deviation is less than 12% when it is close to the detection limit. This method can well meet the needs of factory production control.

Hydrogen sulfide, carbonyl sulfide, sulfur dioxide, carbon disulfide, high column efficiency, good separation, and satisfactory results.


Determination of trace sulfide in process gas. Capillary column Test spectrum: