毛細管柱1：GS-GASPRO  30M*0.32MM

毛細管柱2：FFAP(聚乙二醇類）30m*0.32mm*0.25um

本標準規(guī)定了焦爐煤氣中硫化氫含量的氣相色譜測定的原理、儀器和材料、采樣、分析步驟、結果計算、度和安全注意事項。
本標準適用于焦爐煤氣中硫化氫含量的測定。

定量：外標法

檢測器：FPD火焰光度檢測器

滕州市浩瀚色譜儀器技術服務有限公司，采用浩瀚色譜E公司帶FPD檢測器的GC-型氣相色譜儀測定了焦爐煤氣中H2S的含量,同時用國標的碘滴定法進行試驗數(shù)據(jù)對比。結果表明,本方法分析周期由每樣2 h縮短到10 min左右,且煤氣中H2S的含量在（5～5 000）×10^-6的范圍內(nèi)線性關系良好,準確度高,重現(xiàn)性好,完全滿足不同含量H2S分析要求,是一種簡便快速的分析方法。


氣相色譜法分析焦爐煤氣中H2S 圖片：


Analysis of H2S in Coke Oven Gas by Gas Chromatography
Gas Chromatography Analysis of H2S in Coke Oven Gas Details:

Capillary column 1: GS-GASPRO 30M*0.32MM
Capillary column 2: FFAP (polyethylene glycol) 30m*0.32mm*0.25um

This standard specifies the principles, instruments and materials, sampling, analysis procedures, calculation of results, precision and safety precautions for the determination of hydrogen sulfide in coke oven gas.
This standard applies to the determination of hydrogen sulfide content in coke oven gas.
Quantification: external standard method
Detector: FPD flame photometric detector

Tengzhou Haohao Chromatography Instrument Technology Service Co., Ltd. measured the H2S content in coke oven gas by GC- gas chromatograph with FPD detector from Haohao Chromatography E Co., Ltd., and compared the test data with the national standard iodine titration method. The results show that the analysis period of this method is shortened from 2 h to 10 min, and the H2S content in the gas is in the range of (5～5 000)×10^-6. The linear relationship is good, the accuracy is high, and the reproducibility Well, fully meet the H2S analysis requirements of different levels, it is a simple and rapid analysis method.


Analysis of H2S in Coke Oven Gas by Gas Chromatography